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EAS p-Nitroacetanilide
Pinacol was converted to pinacolone in the experiment at a 15.
60% yield. A low percent yield was expected due to the experimental distillation and experimental separation of the two layers. Some pinacolone could have been trapped in the aqueous layer due to experimental error at separating via a pipet. The IR showed peaks at 2967, 2906, 2871, 2359, 2337, 2173, and 1989. The representative peaks in an IR of pinacolene are present between 3000 and 1700. The NMR when manipulated with a multiple of three, showed the presence of 9 hydrogens at 1.
2 ppm and 3 hydrogens at 2.1 ppm. The typical NMR for pinacolone shows peaks around 20, 40, and 70 ppm due to the electronegativity of the oxygen present in the compound.
The NMR of the organic product is inconsistent with the typical NMR of pinacolone or water. This could potentially be due to a mixture of the two compounds when the NMR was run and is due to the experimental error in the separation of the aqueous and organic layers by pipet. Pinacol was converted to pinacolone in the experiment at a 15.60% yield.
A low percent yield was expected due to the experimental distillation and experimental separation of the two layers. Some pinacolone could have been trapped in the aqueous layer due to experimental error at separating via a pipet. The IR showed peaks at 2967, 2906, 2871, 2359, 2337, 2173, and 1989. The representative peaks in an IR of pinacolene are present between 3000 and 1700. The NMR when manipulated with a multiple of three, showed the presence of 9 hydrogens at 1.2 ppm and 3 hydrogens at 2.1 ppm. The typical NMR for pinacolone shows peaks around 20, 40, and 70 ppm due to the electronegativity of the oxygen present in the compound. The NMR of the organic product is inconsistent with the typical NMR of pinacolone or water. This could potentially be due to a mixture of the two compounds when the NMR was run and is due to the experimental error in the separation of the aqueous and organic layers by pipet.Pinacol was converted to pinacolone in the experiment at a 15.60% yield. A low percent yield was expected due to the experimental distillation and experimental separation of the two layers. Some pinacolone could have been trapped in the aqueous layer due to experimental error at separating via a pipet. The IR showed peaks at 2967, 2906, 2871, 2359, 2337, 2173, and 1989. The representative peaks in an IR of pinacolene are present between 3000 and 1700. The NMR when manipulated with a multiple of three, showed the presence of 9 hydrogens at 1.2 ppm and 3 hydrogens at 2.1 ppm. The typical NMR for pinacolone shows peaks around 20, 40, and 70 ppm due to the electronegativity of the oxygen present in the compound. The NMR of the organic product is inconsistent with the typical NMR of pinacolone or water. This could potentially be due to a mixture of the two compounds when the NMR was run and is due to the experimental error in the separation of the aqueous and organic layers by pipet.Pinacol was converted to pinacolone in the experiment at a 15.60% yield. A low percent yield was expected due to the experimental distillation and experimental separation of the two layers.
Some pinacolone could have been trapped in the aqueous layer due to experimental error at separating via a pipet. The IR showed peaks at 2967, 2906, 2871, 2359, 2337, 2173, and 1989. The representative peaks in an IR of pinacolene are present between 3000 and 1700. The NMR when manipulated with a multiple of three, showed the presence of 9 hydrogens at 1.2 ppm and 3 hydrogens at 2.1 ppm. The typical NMR for pinacolone shows peaks around 20, 40, and 70 ppm due to the electronegativity of the oxygen present in the compound. The NMR of the organic product is inconsistent with the typical NMR of pinacolone or water. This could potentially be due to a mixture of the two compounds when the NMR was run and is due to the experimental error in the separation of the aqueous and organic layers by pipet.Pinacol was converted to pinacolone in the experiment at a 15.60% yield. A low percent yield was expected due to the experimental distillation and experimental separation of the two layers. Some pinacolone could have been trapped in the aqueous layer due to experimental error at separating via a pipet. The IR showed peaks at 2967, 2906, 2871, 2359, 2337, 2173, and 1989. The representative peaks in an IR of pinacolene are present between 3000 and 1700. The NMR when manipulated with a multiple of three, showed the presence of 9 hydrogens at 1.2 ppm and 3 hydrogens at 2.1 ppm. The typical NMR for pinacolone shows peaks around 20, 40, and 70 ppm due to the electronegativity of the oxygen present in the compound. The NMR of the organic product is inconsistent with the typical NMR of pinacolone or water. This could potentially be due to a mixture of the two compounds when the NMR was run and is due to the experimental error in the separation of the aqueous and organic layers by pipet.
Date: May 25,2022